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Characterisation equipment

Dynamic vapour sorption techniques

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nch tone generator crack SPEL features a world-leading Dynamic Vapour sorption facility with access to three Surface Measurement Systems (UK) instruments for operation over relevant temperature (5 – 60 °C) and pressure ranges. Our facility allows us to carry out on-line Raman spectroscopy (785 nm) and electrostatic measurements as well as video imaging as a function of solvent partial pressure, temperature, and time. Typical sample sizes vary from 10 mg to about 100 g depending on the instrument and microbalance used. This allows us a wide range of applications from a typical isotherm measurement of a pharmaceutical powder, BET surface area estimation, to the packaging integrity of a chocolate bar.

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Dry powder particle sizing equipment

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Inverse gas chromatography

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Inverse liquid chromatography

Self-interaction chromatography

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Inverse liquid chromatography

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References:
  1. Quigley, A., Protein Aggregation Behaviour and the Second Virial Coefficient, in Department of Chemical Engineering. 2012, Imperial College London.
  2. Ylä-Mäihäniemi, P. and D.R. Williams, Novel inverse liquid chromatography detector configuration for studying solid–liquid adsorption. Journal of Chromatography A, 2007. 1138(1–2): p. 95-100.
  3. Gorner, T., et al., Inverse Liquid Chromatography Investigation of Adsorption on Heterogeneous Solid Surfaces:  Phenylalanine on Activated Carbon. Langmuir, 2002. 18(22): p. 8546-8552.

Microscopy

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Optical profilometer

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Optical profilometry

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Optical profiler booking procedure

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Photon correlation spectroscopy

Photon correlation spectroscopy / multi-angle dynamic light scattering

Coulter N4 Plus

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N4 PLUS Submicron Particle Size Analysis

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Output Data Analysis Modes:
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Ideal for the rapid identification of different suspensions or emulsions.
For increased accuracy and highly dependable particle size data.

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  • Real time display of instrument status including mode of operation, time remaining in current measurement, and time remaining in entire analysis.
  • Easy-to-read printout of user-defined reports to any printer supported by Windows 3.1.
  • Comparison of results from different runs by overlays.
  • Automatic fluid parameter tables include commonly used fluid refractive index and viscosity data.

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Technical specifications

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  1. Unimodal (cumulants) fit yields mean particle size and standard deviation in nm. Reproducibility: typically better than 3% CV.
  2. Size distribution profile deconvolution algorithm based on CONTIN program yields peak data and bin by bin percentage (intensity or weight) as a function of particle size or molecular weight. Resolution: 17 to 31 size bins, user-selectable. Reproducibility: sample dependent.

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Quartz Crystal Microbalance (QCM)

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Scanning electron microscopy

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Texture analyser

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X-ray diffraction

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Powder x-ray diffractometer

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Processing equipment

Freeze dryer

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HEL auto lab reactor

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